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1.
J Prosthodont ; 2024 May 12.
Artículo en Inglés | MEDLINE | ID: mdl-38734933

RESUMEN

PURPOSE: To evaluate the effect of different printing orientations and post-polymerization time with thermal cycling on the translucency of 3D-printed denture base resins. METHODS: Heat-polymerized (HP) acrylic resin specimens were fabricated and 3D-printed denture base materials (NextDent, ASIGA, FormLabs) were printed with different printing orientations (0, 45, 90 degrees) and subjected to different post-polymerization times (15-, 30-, 60-, and 90-min). All specimens were polished and immersed in distilled water for 1 day at 37°C. CIEDE2000 was used to measure the translucency parameters (TP00) before and after thermal cycling (5000 cycles) recording the color parameters (L*, a*, b*) against a black and white background using a spectrophotometer. k-factors ANOVA followed by post hoc Tukey's test (α = .05) was performed for statistical analysis. RESULTS: The k-factors ANOVA test showed a significant effect of resin material, post-polymerization time, and printing orientation on translucency (p < 0.001). In comparison to HP, all 3D-printed resins showed lower translucency with all post-polymerization times and printing orientation (p < 0.001) except FormLabs resin (p > 0.05). For all 3D-printed resins, the translucency increased, with increasing the post-polymerization time (p < 0.001) and 60- and 90-min showed the highest translucency. For printing orientation, 90 and 45 degrees significantly showed high translucency in comparison to 0 degrees (p < 0.001). FormLabs showed significantly higher translucency when compared with NextDent and ASIGA per respective printing orientation and post-polymerization time. The translucency significantly decreased after thermal cycling for all tested resins (p < 0.001). CONCLUSION: The findings of this study demonstrated that the translucency of 3D-printed resins is influenced by the printing orientation, post-polymerization time, and resin type. As a result, choosing a resin type, and printing orientation, with a longer post-polymerization time should be considered since it may improve the esthetic appearance of the 3D-printed resins.

2.
Eur J Dent ; 17(1): 76-81, 2023 Feb.
Artículo en Inglés | MEDLINE | ID: mdl-35196723

RESUMEN

OBJECTIVE: The current study was designed to assess the bonding strength of EndoSeal MTA and AH Plus sealers after using three irrigation protocols as follows: (1) 17% Ethylenediamine tetraacetic acid, (2) 7% maleic acid, and (3) 37% phosphoric acid. MATERIALS AND METHODS: Push-out bond strength was evaluated for 60 middle root slices of 1-mm thickness each. They were horizontally cut from freshly extracted single-rooted human teeth. A hole in the root canal was made using a carbide round bur of 1.1 mm in diameter in a middle third root slice. Specimens were dipped in 2.5% NaOCl, and then they were grouped into three groups; G1: 17% EDTA, G2: 7% maleic acid, and G3: 37% phosphoric acid as a final irrigant for 3 minutes. Each group was subdivided into two subgroups, according to the type of sealer, either EndoSeal MTA or AH Plus. STATISTICAL ANALYSIS: After the full set of the sealer, the bond strength was evaluated with the push-out test by applying a force to each slice using a plunger with a 1-mm diameter. The one-way Tukey's post hoc test, analysis of variance (ANOVA) test, and Student's t-test were utilized to gather data and statistically evaluate it. RESULTS: The irrigation protocol used exhibited significant influence on the bond strength of EndoSeal MTA and AH Plus sealers. AH Plus sealer subgroups showed the highest bond strength with 7% maleic acid, followed by 37% phosphoric acid, and 17% EDTA. While in the EndoSeal MTA sealer subgroups, the highest bond strength was shown with the 17% EDTA followed by 7% maleic acid and 37% phosphoric acid, respectively. CONCLUSION: The present study revealed that the type of the final irrigant significantly impacts the bond strength of the sealer used. The AH Plus sealer bond strength was improved by using the 7% maleic acid as a final irrigant. In contrast, the EndoSeal MTA sealer showed the best results with the 17% EDTA as a final irrigant.

3.
Materials (Basel) ; 15(24)2022 Dec 19.
Artículo en Inglés | MEDLINE | ID: mdl-36556867

RESUMEN

Denture base fracture is one of the most annoying problems for both prosthodontists and patients. Denture repair is considered to be an appropriate solution rather than fabricating a new denture. Digital denture fabrication is widely spreading nowadays. However, the repair strength of CAD-CAM milled and 3D-printed resins is lacking. This study aimed to evaluate the effect of surface treatment on the shear bond strength (SBS) of conventionally and digitally fabricated denture base resins. One l heat-polymerized (Major base20), two milled (IvoCad, AvaDent), and three 3D-printed (ASIGA, NextDent, FormLabs) denture base resins were used to fabricate 10 × 10 × 3.3 acrylic specimens (N = 180, 30/resin, n = 10). Specimens were divided into three groups according to surface treatment; no treatment (control), monomer application (MMA), or sandblasting (SB) surface treatments were performed. Repair resin was bonded to the resin surface followed by thermocycling (5000 cycles). SBS was tested using a universal testing machine where a load was applied at the resin interface (0.5 mm/min). Data were collected and analyzed using ANOVA and a post hoc Tukey test (α = 0.05). SEM was used for failure type and topography of fractured surfaces analysis. The heat-polymerized and CAD-CAM milled groups showed close SBS values without significance (p > 0.05), while the 3D-printed resin groups showed a significant decrease in SBS (p < 0.0001). SBS increased significantly with monomer application (p < 0.0001) except for the ASIGA and NextDent groups, which showed no significant difference compared to the control groups (p > 0.05). All materials with SB surface treatment showed a significant increase in SBS when compared with the controls and MMA application (p < 0.0001). Adhesive failure type was observed in the control groups, which dramatically changed to cohesive or mixed in groups with surface treatment. The SBS of 3D-printed resin was decreased when compared with the conventional and CAD-CAM milled resin. Regardless of the material type, SB and MMA applications increased the SBS of the repaired resin and SB showed high performance.

4.
J Prosthodont ; 31(3): 257-265, 2022 Mar.
Artículo en Inglés | MEDLINE | ID: mdl-34318547

RESUMEN

PURPOSE: This study aimed to evaluate the repair strength of a newly introduced repair technique involving zero-gap repair width. MATERIALS AND METHODS: A total of 36 rectangular prism specimens with dimensions of 64 × 10 × 3.3 mm were prepared from heat-polymerized acrylic resin. Nine specimens were kept intact. The other specimens were sectioned into halves and modified to create repair gaps of 2.5-mm beveled (2.5B) as control, 0-mm beveled (ZB), and 0-mm inverse bi-beveled (ZIBB). The ZIBB group was prepared with a V-shaped internal groove on both halves (repair tunnel), while the intaglio and cameo surfaces were kept intact except for two small holes at the cameo surface for repair resin injection. The 2.5B and ZB groups were repaired conventionally while the ZIBB group was repaired by injecting repair resin into the tunnel through one of the holes until excess material oozed from the other hole. Repaired specimens were thermally cycled at 5 and 55°C for 10,000 cycles with 1 min dwell time. A 3-point bending test was conducted using a universal testing machine for flexural strength and elastic modulus measurement. Kruskal-Wallis/Mann-Whitney tests and ANOVA/post hoc Tukey tests were applied for data analysis (α = 0.05). RESULTS: The flexural strength of repaired specimens was substantially lower than that of intact specimens, and significant differences were present between repaired groups (p ˂ 0.05). ZB and ZIBB had higher flexural strength (p ˂ 0.001) and elastic modulus (p ˂ 0.05) than 2.5B. Among the ZB and ZIBB groups, ZB showed the highest flexural strength, and ZIBB had the highest elastic modulus. CONCLUSION: The closed repair technique improved the flexural strength and elastic modulus of repaired acrylic denture base.


Asunto(s)
Bases para Dentadura , Reparación de la Dentadura , Reparación de la Dentadura/métodos , Ensayo de Materiales , Docilidad , Polimetil Metacrilato , Propiedades de Superficie
5.
J Prosthet Dent ; 127(1): 174-183, 2022 Jan.
Artículo en Inglés | MEDLINE | ID: mdl-33190862

RESUMEN

STATEMENT OF PROBLEM: Whether the addition of different antifungal nanoparticles to denture base materials may affect physical or esthetic properties of the resulting nanocomposite is unclear. PURPOSE: The purpose of this in vitro study was to determine how a new method of adding antifungal nanofiller affects the properties of the processed nanocomposite denture base material. MATERIAL AND METHODS: Heat-polymerized acrylic resin specimens were prepared according to each test specification. Zirconium dioxide nanoparticles (ZrO2NPs) and silver nanoparticles (AgNPs) were added in 0.5, 1.0, and 1.5% of acrylic resin powder. The specimens were divided into 2 groups according to the acrylic resin packing method: 1 layer packed conventionally in one step and 2 layers packed in 2 steps, first with unmodified acrylic resin and then by a thin layer of modified acrylic resin before the final closure. The control group was made of unaltered acrylic resin in 1 step. Flexural strength (FS), translucency, and surface roughness (Ra) were measured. A microbial assay was performed by using the direct culture and slide count methods. Three-way ANOVA and Tukey post hoc tests were used to identify statistical differences among groups (α=.05). RESULTS: The addition of ZrO2NPs and AgNPs in the 1- or 2-layer specimens reduced Candida albicans adhesion (P<.001). In the 1- and 2-layer specimens, FS significantly increased with ZrO2NPs. AgNPs decreased FS only in the 1-layer specimen (P<.001). Surface roughness was not changed for the 1- and 2-layer specimens with ZrO2NPs or the 1-layer specimen with 0.5% AgNPs (P>.05), while other AgNP groups exhibited increased surface roughness (P<.001). AgNPs significantly lowered translucency in the 1- and 2-layer specimens (P<.001), while ZrO2NPs decreased translucency only in the 1-layer specimen (P<.001). CONCLUSIONS: The addition of ZrO2NPs in the double-layer technique decreased Candida adhesion and improved FS without affecting surface roughness, while AgNPs decreased Candida adhesion and FS and increased surface roughness. Both nanofillers decreased the translucency except 0.5% ZrO2NPs, which did not change translucency when applied in 2 layers.


Asunto(s)
Resinas Acrílicas , Nanopartículas del Metal , Bases para Dentadura , Estética Dental , Ensayo de Materiales , Polimetil Metacrilato , Plata , Propiedades de Superficie
6.
Int J Biomater ; 2021: 6668577, 2021.
Artículo en Inglés | MEDLINE | ID: mdl-33927766

RESUMEN

OBJECTIVES: This study aimed to evaluate denture cleanser effects on color stability, surface roughness, and hardness of PMMA denture base resin reinforced with nano-ZrO2. MATERIALS AND METHODS: A total of 420 specimens were fabricated of unreinforced and nano-ZrO2 reinforced acrylic resin at 2.5% and 5%, resulting in 3 main groups. These groups were further subdivided (n = 10) according to immersion solution (distilled water, Corega, sodium hypochlorite, and Renew) and immersion duration. Surface roughness, hardness, and color were measured at baseline (2 days-T 0) in distilled water and then after 180 and 365 days of immersion (T 1 & T 2) in water or denture cleansing solutions. Data was collected and analyzed using two-way ANOVA followed by Bonferroni post hoc test (α = 0.05). RESULTS: Surface roughness increased significantly after denture cleanser immersion of unmodified and nano-ZrO2-modified PMMA materials while hardness decreased (P < 0.001). The denture cleansers significantly affected the color of both PMMA denture bases (P < 0.001). The immersion time in denture cleansers significantly affected all tested properties (P < 0.001). Within denture cleansers, NaOCl showed the highest adverse effects (P < 0.05) while Renew showed the least adverse effects. CONCLUSION: Denture cleansers can significantly result in color change and alter the surface roughness and hardness of denture base resin even with ZrO2 nanoparticles addition. Therefore, they should be carefully used.

7.
J Prosthodont ; 30(3): 235-244, 2021 Mar.
Artículo en Inglés | MEDLINE | ID: mdl-32783226

RESUMEN

PURPOSE: The additions of zirconium oxide nanoparticles (nano-ZrO2 ) to denture base materials have produced nanocomposites with satisfactory properties, although there is a lack of research investigating the effects of denture cleansers on these materials. This study aimed to evaluate the effect of denture cleansers on the flexural strength of denture base materials modified with nano-ZrO2 . MATERIALS AND METHODS: A total of 270 specimens were fabricated from pure and nano-ZrO2 reinforced acrylic resins at 2.5% and 5%, resulting in 3 main groups. The groups were further divided into subgroups (n = 10) according to immersion solution (distilled water, Corega, sodium hypochlorite, and Renew) and immersion duration. Flexural strength was measured at baseline (T0 ) in distilled water and after 180 and 365 days of immersion (T1 and T2 ) in denture cleansers. Data were collected and analyzed using repeated measure ANOVA and Bonferroni post hoc tests (α = 0.05). RESULTS: The flexural strength of the nano-ZrO2 modified denture base material decreased significantly after immersion in different denture cleansers at different immersion durations in comparison to baseline (T0 ) (p < 0.001). Sodium hypochlorite showed the highest reduction in flexural strength followed by Corega, while Renew cleansing solution resulted in the least change. CONCLUSION: Denture cleansers can significantly affect the flexural strength of nano-ZrO2 modified denture base materials and thus should be used cautiously.


Asunto(s)
Bases para Dentadura , Nanopartículas , Limpiadores de Dentadura , Resistencia Flexional , Ensayo de Materiales , Polimetil Metacrilato , Propiedades de Superficie
8.
J Clin Exp Dent ; 12(4): e354-e362, 2020 Apr.
Artículo en Inglés | MEDLINE | ID: mdl-32382385

RESUMEN

BACKGROUND: The purpose of this study was to evaluate the effect of aging process on the tensile strength (TS) of repaired acrylic denture base using ZrO2 nanoparticles (nano-ZrO2)-reinforced autopolymerized resin. MATERIAL AND METHODS: A total of 240 heat-polymerized acrylic resin specimens (n=10) were prepared and sectioned creating 2 mm-repair-gap. Autopolymerized acrylic resin, pure and modified with 2.5, 5, and 7.5wt% nano-ZrO2 were used for specimens repair. TS of repaired specimens were measured using the universal testing machine after water immersion at 37oC for 2, 7 and 30 days. At each time interval, half the immersed specimens underwent thermo-cycling aging process (5000 cycles at 5/55°C) before TS testing. One-way ANOVA and Tukey-Kramer multiple-comparison tests were used for data analysis at α=0.05. RESULTS: Aging process for all groups showed significant differences in TS between unreinforced and nano-ZrO2 reinforced groups (p<0.05). Within immersed nano-ZrO2-reinforced specimens, 5% group immersed for 30-days showed the highest significant TS value (p<0.05). With regards to thermocycling, 5% group showed the highest TS values after 2-days and 30-days groups while after 7-days, significant differences were found between 2.5% group and 5% and 7.5% groups (p<0.05). SEM images analysis displayed the ductile fracture type for nano-ZrO2 reinforced groups. CONCLUSIONS: In summary, 5.0%-nano-ZrO2 addition to repair resin showed an improvement in tensile strength of repaired acrylic resin with different aging processes. Key words:Acrylic resins, denture repair, tensile strength, thermocycling, water storage, zirconium oxide nanoparticle.

9.
Dent Mater J ; 39(3): 471-482, 2020 Jun 05.
Artículo en Inglés | MEDLINE | ID: mdl-32092720

RESUMEN

This study assessed the impact of surface treatments and repair resin reinforcement with zirconium oxide nano-particles (nano-ZrO2) on flexural strength (FS) of repaired denture base. A total of 320 heat-polymerized acrylic resin specimens were prepared and sectioned creating 2-mm gap. According to repair surface treatment, specimens were distributed into four groups: I) methyl methacrylate (M); II) alumina-blasted (AB); III) AB+silane coupling agent (SC); and IV) AB+methacrylate based composite bonding agent (MA). Groups were subdivided into 4 (n=20) according to nano-ZrO2 concentration (0, 2.5, 5, 7.5 wt%). Half the specimens were thermo-cycled before testing. FS was determined by three-point bending test. Statistical analysis was done using ANOVA and Tukey-Kramer multiple comparison tests, with α=0.05. Alumina-blasting+(SC) or (MA) significantly increased FS of repaired specimens compared to control (p<0.05). All surface-treated specimens combined with nano-ZrO2 reinforced repair resin significantly increased FS.


Asunto(s)
Bases para Dentadura , Polimetil Metacrilato , Resinas Acrílicas , Resistencia Flexional , Ensayo de Materiales , Docilidad , Propiedades de Superficie
10.
J Prosthodont ; 28(6): 684-691, 2019 Jul.
Artículo en Inglés | MEDLINE | ID: mdl-31150133

RESUMEN

PURPOSE: To evaluate the effect of repair gap width on the flexural strength and impact strength of a repaired acrylic denture with and without thermal cycling. MATERIALS AND METHODS: A total of 240 heat-polymerized acrylic resin specimens were fabricated in dimensions of 65 × 10 × 2.5 ± 0.2 mm and 55 × 10 × 10 ± 0.2 mm for flexural strength and impact strength testing, respectively. All specimens were sectioned into halves then divided into 6 groups according to repair gap width (n = 10). The repair gap of the control group was 2.5 mm at the base, while the repair gaps of the test groups were prepared as 2.0, 1.5, 1.0, 0.5, and 0 mm at the base. All specimens were prepared with a 45° bevel joint. Each specimen was placed into the mold that retained the original length of the specimen and modified only the repair gap, which was packed with repair resin. After polymerization, specimens were finished and polished, and half of the specimens were thermal cycled for 5000 cycles. Three-point bending test and Charpy impact test were used to determine the flexural strength and impact strength, respectively. ANOVA and Tukey's HSD test were used for statistical analysis, where α was set at 0.05. RESULTS: Decreasing repair gap significantly increased the flexural strength in comparison to control group (p < 0.05); 0.5-mm repair gap showed the highest flexural strength values. Changing the repair gap significantly increased the impact strength of groups 2.0- and 1.5-mm (p < 0.05). Thermal cycling significantly decreased the flexural strength of all tested groups as well as impact strength for groups with wide repair gaps (2.5-, 2.0-, and 1.5-mm) (p < 0.05), while other tested groups had nonsignificant effect on impact strength (p > 0.05). CONCLUSION: Decreasing repair gap increased the flexural and impact strengths of repaired acrylic resin. A repair gap of 0-, 0.5-, or 1.0-mm with beveled repair surface is recommended to improve repair strength and overcome the drawbacks of increased amounts of autopolymerized repair resin.


Asunto(s)
Bases para Dentadura , Reparación de la Dentadura , Resinas Acrílicas , Análisis del Estrés Dental , Ensayo de Materiales
11.
Int J Dent ; 2019: 2489393, 2019.
Artículo en Inglés | MEDLINE | ID: mdl-30809260

RESUMEN

This study is aimed at evaluating the hybrid reinforcement effects of zirconium oxide nanoparticles (nano-ZrO2) and glass fibers (GFs) at different ratios on the flexural and impact strengths of a polymethylmethacrylate (PMMA) denture base. A total of 160 specimens were fabricated from heat-polymerized acrylic resins using the water bath technique. For the control group, the specimens did not receive any additions; for the test group, different concentrations of nano-ZrO2/GFs at 5% of the PMMA polymer were added. The concentrations of nano-ZrO2/GFs were as follows: 5%-0%, 4%-1%, 3%-2%, 2.5%-2.5%, 2%-3%, 1%-4%, and 0%-5%. The flexural strength was measured using the three-point bending test. The impact strength was measured using the Charpy impact test. Results were tabulated and analyzed using one-way analysis of variance (ANOVA) and the Tukey-Kramer multiple comparison test (p ≤ 0.05). The flexural and impact strengths of PMMA-nano-ZrO2 + GF composites were significantly improved when compared with those of pure PMMA (p < 0.05). The maximum flexural strength (94.05 ± 6.95 MPa) and impact strength (3.89 ± 0.46 kJ/m2) were obtained with PMMA (2.5%)/nano-ZrO2 + 2.5% GF mixtures and could be used for removable prosthesis fabrication.

12.
Int J Health Sci (Qassim) ; 12(5): 66-69, 2018.
Artículo en Inglés | MEDLINE | ID: mdl-30202410

RESUMEN

OBJECTIVE: The objective of this study was to measure the push-out bond strength of three types of mineral trioxide aggregate (MTA) materials in root dentin. METHODS: The study was carried out at the College of Dentistry, Imam Abdulrahman Bin Faisal University from March 2014 to January 2015. Thirty extracted maxillary central incisors were selected, instrumented, irrigated, and randomly assigned into three groups (n = 10): Group 1 - Ortho MTA; Group 2 - MTA Angelus; and Group 3 - ProRoot MTA. Materials were mixed following the manufacturers' recommendations and canals were filled. Teeth were stored in distilled water for 6 months. The push-out bond strength was evaluated using 2-mm thick coronal root sections. The data were analyzed with one-way ANOVA and Tukey-Kramer multiple comparison tests statistically significant at P < 0.05. RESULTS: The mean bond strength values were 68.69 ± 29.63 MPa for Ortho MTA, 42.54 ± 32.78 MPa for MTA Angelus, and 72.75 ± 26.27 MPa for ProRoot MTA groups. There were no significant differences between the bond strengths of tested materials (P > 0.05). CONCLUSION: Ortho MTA, MTA Angelus, and ProRoot MTA materials showed similar push-out bond strength values in root dentin.

13.
Dent Mater J ; 37(5): 746-753, 2018 Sep 30.
Artículo en Inglés | MEDLINE | ID: mdl-29925729

RESUMEN

The current study evaluated the effects of autoclave polymerization both with and without glass fiber (GF) reinforcement on the surface roughness and hardness of acrylic denture base material. Ninety disc specimens (30×2.5 mm) were prepared from Vertex resin and divided according to polymerization techniques into a water bath, short and long autoclave polymerization groups. Tested groups were divided into three subgroups according to the GF concentration (0, 2.5, and 5 wt%). Profilometer and Vickers hardness tests were performed to measure surface roughness and hardness. ANOVA and Tukey-Kramer multiple comparison tests analyzed the results, and p≤0.05 was considered statistically significant. Autoclave polymerization significantly decreased the surface roughness and increased the hardness of acrylic resin without GF reinforcement (p<0.05). However, 5 wt% GF addition significantly increased surface roughness and decreased hardness of the autoclave polymerized denture base resin (p<0.05). Surface properties of Polymethyl methacrylate (PMMA) denture base material improved with autoclave polymerization and negatively affected with GFs addition.


Asunto(s)
Resinas Acrílicas/química , Materiales Dentales/química , Bases para Dentadura , Vidrio/química , Polimetil Metacrilato/química , Pruebas de Dureza , Ensayo de Materiales , Polimerizacion , Propiedades de Superficie
14.
Int J Nanomedicine ; 13: 283-292, 2018.
Artículo en Inglés | MEDLINE | ID: mdl-29391789

RESUMEN

BACKGROUND: Polymethyl methacrylate (PMMA) is widely used for the fabrication of removable prostheses. Recently, zirconium oxide nanoparticles (nano-ZrO2) have been added to improve some properties of PMMA, but their effect on the optical properties and tensile strength are neglected. OBJECTIVE: The aim of this study was to investigate the effect of nano-ZrO2 addition on the translucency and tensile strength of the PMMA denture base material. MATERIALS AND METHODS: Eighty specimens (40 dumbbell-shaped and 40 discs) were prepared out of heat-polymerized acrylic resin and divided into four groups per test (n=10). The control group for each test included unreinforced acrylic, while the test groups were reinforced with 2.5, 5, and 7.5 wt% nano-ZrO2. Acrylic resin was mixed according to manufacturer's instructions, packed, and processed by conventional method. After polymerization, all specimens were finished, polished, and stored in distilled water at 37°C for 48±2 hours. Tensile strength (MPa) was evaluated using the universal testing machine while the specimens' translucency was examined using a spectrophotometer. Statistical analysis was carried out by SPSS using the paired sample t-test (p≤0.05). A scanning electron microscope was used to analyze the morphological changes and topography of the fractured surfaces. RESULTS: This study showed that the mean tensile strength of the PMMA in the test groups of 2.5%NZ, 5%NZ, and 7.5%NZ was significantly higher than the control group. The tensile strength increased significantly after nano-ZrO2 addition, and the maximum increase seen was in the 7.5%NZ group. The translucency values of the experimental groups were significantly lower than those of the control group. Within the reinforced groups, the 2.5%NZ group had significantly higher translucency values when compared to the 5%NZ and 7.5%NZ groups. CONCLUSION: The addition of nano-ZrO2 increased the tensile strength of the denture base acrylic. The increase was directly proportional to the nano-ZrO2 concentration. The translucency of the PMMA was reduced as the nano-ZrO2 increased. CLINICAL SIGNIFICANCE: Based on the results of the current study, the tensile strength was improved with different percentages of nano-ZrO2 additions. However, translucency was adversely affected. Therefore, it is important to determine the appropriate amount of reinforcing nano-ZrO2 that will create a balance between achieved properties - mechanical and optical.


Asunto(s)
Bases para Dentadura , Nanopartículas/química , Polimetil Metacrilato/química , Circonio/química , Resinas Acrílicas/química , Humanos , Ensayo de Materiales , Polimerizacion , Resistencia a la Tracción
15.
Int J Nanomedicine ; 11: 5633-5643, 2016.
Artículo en Inglés | MEDLINE | ID: mdl-27822041

RESUMEN

BACKGROUND: Repeated fracture of the denture base is a common problem in prosthodontics, and it represents a nuisance and a time sink for the clinician. Therefore, the possibility of increasing repair strength using new reinforcement materials is of great interest to prosthodontists. AIM OF THE STUDY: This study aimed to evaluate the effects of incorporation of zirconia nanoparticles (nano-ZrO2) on the flexural strength and impact strength of repaired polymethyl methacrylate (PMMA) denture bases. MATERIALS AND METHODS: One hundred eighty specimens of heat-polymerized acrylic resin were fabricated (90 for each test) and divided into three main groups: one control group (intact specimens) and two groups divided according to surface design (45° bevels and butt joints), in which specimens were prepared in pairs to create 2.5 mm gaps. Nano-ZrO2 was added to repair resin in 2.5 wt%, 5 wt%, and 7.5 wt% concentrations of acrylic powder. A three-point bending test was used to measure flexural strength, and a Charpy-type test was used to measure impact strength. Scanning electron microscopy was used to analyze the fracture surfaces and nano-ZrO2 distribution. The results were analyzed with a paired sample t-test and an unpaired t-test, with a P-value of ≤0.05 being significant. RESULTS: Incorporation of nano-ZrO2 into the repair resin significantly increased flexural strength (P<0.05). The highest value was found in the bevel group reinforced with 7.5% nano-ZrO2, whereas the lowest value was found in the butt group reinforced with 2.5% nano-ZrO2. The impact strength values of all repaired groups were significantly lower than those of the control group (P<0.05). Among repaired groups, the higher impact strength value was seen in the butt group reinforced with 2.5% nano-ZrO2. The bevel joint demonstrated mainly cohesive failure, whereas the butt joint demonstrated mainly adhesive failure. CONCLUSION: Incorporation of nano-ZrO2 into the repair resin improved the flexural strength of repaired denture bases, whereas it decreased impact strength, especially with high nano-ZrO2 concentrations.


Asunto(s)
Materiales Dentales/química , Bases para Dentadura , Reparación de la Dentadura , Nanopartículas/administración & dosificación , Polimetil Metacrilato/química , Circonio/química , Resinas Acrílicas/química , Humanos , Ensayo de Materiales , Nanopartículas/química , Polimerizacion , Estrés Mecánico , Propiedades de Superficie , Circonio/administración & dosificación
16.
Int J Dent ; 2016: 7094056, 2016.
Artículo en Inglés | MEDLINE | ID: mdl-27366150

RESUMEN

Objective. The aim of this study was to evaluate the effect of incorporation of glass fiber, zirconia, and nano-zirconia on the transverse strength of repaired denture base. Materials and Methods. Eighty specimens of heat polymerized acrylic resin were prepared and randomly divided into eight groups (n = 10): one intact group (control) and seven repaired groups. One group was repaired with autopolymerized resin while the other six groups were repaired using autopolymerized resin reinforced with 2 wt% or 5 wt% glass fiber, zirconia, or nano-zirconia particles. A three-point bending test was used to measure the transverse strength. The results were analyzed using SPSS and repeated measure ANOVA and post hoc least significance (LSD) test (P ≤ 0.05). Results. Among repaired groups it was found that autopolymerized resin reinforced with 2 or 5 wt% nano-zirconia showed the highest transverse strength (P ≤ 0.05). Repairs with autopolymerized acrylic resin reinforced with 5 wt% zirconia showed the lowest transverse strength value. There was no significant difference between the groups repaired with repair resin without reinforcement, 2 wt% zirconia, and glass fiber reinforced resin. Conclusion. Reinforcing of repair material with nano-zirconia may significantly improve the transverse strength of some fractured denture base polymers.

17.
J Hand Microsurg ; 3(2): 45-50, 2011 Dec.
Artículo en Inglés | MEDLINE | ID: mdl-23204767

RESUMEN

The incidence of hand burns in children is high. In the overall cases of body burns, hand and wrist burns account for about 39%. They may constitute a part of a larger burn of the body, or an isolated injury of the hand and wrist. The choice between early and late escharectomy and skin covering is still a matter of debate. Two cases of deep burns of the hands are presented in this report. The report shows a new way to close the residual wounds of deep burns.

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